glutathione strucutre Oxidized (GSSG), Hydrogen acceptor (CAS 27025-41-8) All Skin Types

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The residue was purified by silica gel column chromatography (80:18:2 CHCl 3 /CH 3 OH/NH 4 OH) to afford guanidine 102 (645 mg, 37% and 640 mg, 37% impure) as a yellow solid: 1 H NMR (400 MHz, CD 3 OD) 7.70 (dd, J=9.0, 4.3 Hz, 2H), 7.66 (s, 1H), 7.61 (s, 1H), 7.39-7.31 (m, 4H), 7.11 (d, J=8.4 Hz, 2H), 4.48 (t, J=7.6 Hz, 1H), 3.30-3.22 (m, 3H), 3.06 (dd, J=13.8, 8.9 Hz, 1H), 2.83 (t, J=7.2 Hz, 2H), 2.57 (t, J=7.9 Hz, 2H), 2.32 (dd, J=10.5, 7.6 Hz, 2H), 2.23 (s, 6H), 1.86-1.74 (m, 4H), 1.73-1.64 (m, 2H), 1.32 (s, 9H)